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PTECH+™52: Torque-Turn Test Report

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Torque-Turn Test Report

PTECH+™52 Connection

Test Location
Mechanical Testing Services (MTS)20530 Stokes Road

Waller, Texas

Date of TestApril 27 & 28, 2023

Prepared ByJackson DeBrayRussell Werner

Report DateAugust 30, 2023

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PTech+™ 52 Torque-Turn Test MTS, Waller-Tx, 27-April-2023 Table of ContentsIntroduction ........................................................................................................................................................... 1Test Overview and Objectives ............................................................................................................................... 11. Multi-Cycle Make and Break Test .................................................................................................................. 12. Torque to Yield Test ....................................................................................................................................... 1Tool Joint Samples (Traceability) ........................................................................................................................... 2Hydraulic Bucking Unit ........................................................................................................................................... 2Test Procedure, Multi-Cycle Torque Test ............................................................................................................... 2Test Procedure, Torque to Yield Test ..................................................................................................................... 3Test Results, Multi-Cycle Torque Test .................................................................................................................... 4Test Results, Torque to Yield Test .......................................................................................................................... 5Summary and Comments ...................................................................................................................................... 5Appendix A (Tool Joint Data, Mechanical and Chemistry) ......................................................................... (1 Page)Appendix B (Certificate of Calibration, Hydraulic Bucking Unit) ............................................................... (2 Pages)Appendix C (Test Data, Multi-Cycle Torque Test) ..................................................................................... (1 Page)Appendix D (Torque to Yield Curve) .......................................................................................................... (1 Page)Attachment A (Photographs) .................................................................................................................... (6 Pages)Attachment B (MTS Torque-Turn Curves, Multi-Cycle and Torque to Yield, Makeup and Breakout)Tool Joint Set A (torque-turn to yield test not performed) ................................................................. (24 pages)Tool Joint Set B ...................................................................................................................................... (8 pages)Tool Joint Set C..................................................................................................................................... (32 pages)Tool Joint Set D .................................................................................................................................... (28 pages)

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PTech+™ 52 Torque-Turn Test MTS, Waller-Tx, 27-April-2023 Page 1 of 5 Introduction: Torque tests were performed on four PTech+™ 52 tool joint sets. For reporting purposes, the tool joint sets were labeled Set A, B, C and D. All tests were performed at Mechanical Testing Services (MTS), located at 20530 Stokes Road in Waller, Texas. Applied torque and turn data was recorded for all makeup and breakout cycles using the facility’s McCoy RP7022 hydraulic bucking unit. Jet-Lube KOPR EXT FF 1.0 thread compound (1.0 friction factor) was used for all torque cycles performed on all tool joint sets. Test Overview and Objectives: Two types of torque tests were performed on each tool joint set; multi-cycle makeup and breakout test and torque to yield test. 1. Multi-Cycle Make and Break Test: (Makeup Torque = 60% and 70% of Calculated Torsional Yield) Multiple makeup and breakout cycles were performed on each tool joint set. An aim makeup torque value of 54,800 ft-lb (60% of calculated torsional yield) was used for the first three torque cycles applied to tool joint Set A. An aim makeup torque value of 63,980 ft-lb (70% of calculated torsional yield) was used for all subsequent torque cycles applied to tool joint Set A. An aim makeup torque value of 54,800 ft-lb (60% of calculated torsional yield) was used for all torque cycles applied to tool joint Set B, Set C and Set D. Torque-turn data (makeup and breakout) was recorded for all cycles. Due to field reported instances of connection loosening while oscillating/rocking the drill string during slide drilling mode, this test was performed to document the connection breakout to makeup torque ratio. After the initial makeup cycle, a punch mark was applied on the box and pin tool joint OD. The punch marks were used to document relative position of the box and pin shoulders at the end of each subsequent makeup cycle. The goal was to perform multiple make and break cycles until 3 consecutive cycles were achieved with no relative change in position of the mating shoulders at makeup. The data would be used to determine: - Does relative position of shoulders stabilized after a given number of make and break cycles - Is relative shoulder position related to the connection breakout to makeup torque ratio - Does relative position of shoulders stabilize at less make and break cycles using a makeup torque value equal to 70% of connection torsional yield versus 60% of connection torsional yield. 2. Torque to Yield Test: A torque to yield test was performed on tool joint Set B, C and D. Applied torque and turn data (makeup and breakout) was recorded during the test. The test was performed to validate connection calculated torsional yield. A torque to yield test was not performed on tool joint Set A due to pin connection thread damage (galled flanks) sustained during the multi-cycle make and break test. It was decided the thread damage would affect the torque to yield test and produce misleading (inaccurate) results. The torque to yield test was the final test performed on the tool joint sets.

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PTech+™ 52 Torque-Turn Test MTS, Waller-Tx, 27-April-2023 Page 2 of 5 Tool Joint Samples: All tool joints were randomly selected from TSC-DP inventory. The tool joints were new, manufactured by JST, and had received a 3-cycle connection break-in by JST at time of manufacture. The tool joints were 6.625” OD by 3.750” ID, manganese phosphate coated, and manufactured to specification TSC-0004 Rev 2, with 135 ksi specified minimum yield strength. Tool joint mechanical properties and chemistry reported in the JST quality documentation package are shown in Appendix A. JST traceability markings stamped on the tool joint OD were recorded and are shown in the below table. JST Tool Joint Identification Stamping Tool Joint Tool Joint Serial No. Heat No. Heat Treat Lot No. Set A Pin 22RN03541 E12209480XX D230169 Box 22RP03430 E22211196AX D230406 Set B Pin 22RN03739 E12209480XX D230154 Box 22RP03210 E22211196AX D230401 Set C Pin 22RN01259 E22209327XX D230109 Box 22RP02780 E22211197XX D230265 Set D Pin 22RN03727 E12209480XX D230153 Box 22RP02784 E22211197XX D230265 Hydraulic Bucking Unit: All make and break cycles were performed on MTS’s McCoy RP7022 hydraulic bucking unit. The unit is a continuous drive (rotational) system with a maximum applied torque capacity of 105,000 ft-lb. Work pieces are positioned horizontally in the unit. The driving chuck is located in the unit’s head stock and the static chuck (back-up tong) is located in the unit’s tail stock. The drive chuck and static chuck each have six hydraulic ram cylinders that grip the work pieces. The unit is equipped with a data acquisition system that monitors applied torque and turns. The unit has a display screen that plots a torque-turn graph during progression of the makeup and breakout cycle. Refer to Appendix B for hydraulic bucking unit certificate of torque calibration provided by MTS. Test Procedure, Multi-Cycle Make and Break Test: (Makeup Torque = 60% and 70% of Torsional Yield) 1. Prior to start of test, a dimensional and visual inspection was performed on each connection and the data recorded. All connections met new product dimensional requirements. Refer to Appendix C for inspection report. Tool joints were paired in sets and labeled A, B, C and D. Set pairing was maintain during all torque cycles. 2. Test Sequence: 2.1. Box and pin connections were thoroughly cleaned and Jet-Lube KOPR EXT FF 1.0 thread compound applied to each connection. 2.2. Connections were mated together by hand at a work station and manually tightened using a strap tong. 2.3. The tool joint set was loaded in the hydraulic bucking unit with the pin tool joint positioned in the head stock (drive chuck) and the box tool joint positioned in the tail stock (static chuck). The tool joints were positioned such that the hydraulic bucking unit ram cylinders gripped over the tool joint body, away from the connection.

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PTech+™ 52 Torque-Turn Test MTS, Waller-Tx, 27-April-2023 Page 3 of 5 2.4. The hydraulic bucking unit was preset to apply a peak makeup torque value established by TSC-DP. An aim makeup torque value of 54,800 ft-lb (60% of TY)was used for all makeup cycles performed on tool joint Sets B, C and D. An aim makeup torque value of 54,800 ft-lb (60% of TY) was used for the first three makeup cycles performed on tool joint Sets A. An aim makeup torque value of 63,980 ft-lb (70% of TY) was used for all subsequent cycles applied to tool joint Set A. The 60% TY makeup torque value represents TSC-DP’s recommended makeup torque and the 70% TY value represents TSC-DP’s maximum makeup torque (both values based on using a 1.0 friction factor thread compound). All applied torque cycles were performed using a speed of approximately 1.5 RPM. 2.5. After application of the initial makeup torque cycle, the tail stock chuck was released and positioned away from the box tool joint. TSC-DP applied a punch mark on the pin and box tool joint OD adjacent to the RSC bevel runout. The punch marks were positioned in axial alignment and used to document relative position of the connection shoulders at the end of each subsequent makeup torque cycle. (Note, tool joint Set C punch marks were applied after the third makeup cycle.) 2.6. The hydraulic bucking unit tail stock was repositioned over the box tool joint and the connection set broken apart. 2.7. The tool joint set was separated and each connection visually inspected for damage that might interfere with subsequent torque cycles. The examination included inspection of threads using a brass pick tool. After visual inspection, fresh thread compound was applied to the connections, and the tool joint set mated by hand and tightened using a strap tong. 2.8. The hydraulic bucking unit was used to reapply the same makeup torque value applied in Step 2.4. Step 2.3 and 2.4 procedures were repeated during reapplication of makeup torque. After each application of makeup torque, the hydraulic bucking unit tail stock was released and positioned away from the box tool joint. A metal Pi taper was used to measure the radial distance between the two punch marks and the data recorded. 2.9. Steps 2.6 through 2.8 were repeated for subsequent make and break cycles until three consecutive cycles were achieved with no change in relative position of the punch marks. 2.10. After achieving three consecutive cycles with no change in relative position of the punch marks, the tool joint set was separated, thoroughly cleaned, and visually inspected for damage. A dimensional inspection of select connection features was performed to ensure the connections were in good condition and suitable for performing a torque to yield test. Refer to Appendix D for inspection report performed at the conclusion of the multi-cycle torque test. Test Procedure, Torque to Yield: (Tool Joint Set B, C and D) 1. Fresh thread compound was applied to each connection and the tool joint set manually tightened using a strap tong. Tool joint set paring from the multi-cycle torque test was maintained for the torque to yield test. 2. The tool joint set was loaded in the hydraulic bucking unit with the pin tool joint positioned in the head stock (drive chuck) and the box tool joint positioned in the tail stock (static chuck). The tool joints were positioned such that the hydraulic tong unit rams gripped over the tool joint body, away from the connection. 3. Makeup torque was applied at a rate of approximately 1.0 RPM. The hydraulic bucking unit display (torque versus turn graph) was monitored during the makeup cycle. The test was concluded once

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PTech+™ 52 Torque-Turn Test MTS, Waller-Tx, 27-April-2023 Page 4 of 5 the display indicated the connection had yielded, as evident by a change in the slope of the torque-turn curve and when the applied makeup torque exceeded the calculated torsional yield of the connection. Torque-turn data (makeup and breakout) was recorded for each tool joint set. Test Results, Multi-Cycle Make and Break Test: (Makeup Torque = 60% and 70% of Torsional Yield) No test abnormalities occurred during any make and break cycles. A summary of breakout to makeup torque ratio and change in relative position of connection shoulders is shown in the below table. Data for each individual make and break cycle is shown in Appendix E. Refer to Attachment B for MTS torque-turn curves for individual makeup and breakout cycles. Internal Ratio Relative Position Tool Shoulder Breakout to Makeup Torque of Shoulders at Joint Gap Total (%) Last Makeup Cycle Set (in) Cycles Min Max Avg (in) A 0.0103 12 76.8 81.2 79.5 20/32 B 0.0089 3 80.9 81.9 81.4 2/32 C 0.0095 15 75.9 82.0 78.5 5/32 D 0.0086 13 73.9 80.4 75.8 12/32 Internal shoulder gap based on connection lengths prior to start of test (see Appendix C inspection report) Set B, C and D aim makeup torque, all cycles = 54,800 ft-lb (60% of TY and 1.0 FF) Set A aim makeup torque, cycle 1 thru 3 = 54,800 ft-lb (60% of TY and 1.0 FF) Set A aim makeup torque, cycle 4 thru 12 = 63,980 ft-lb (70% of TY and 1.0 FF) The multi-cycle test performed on tool joint Sets A, C and D was successful in reaching the goal of three consecutive makeup cycles with no change in relative position of the shoulders. Due to constraint in allotted time at the test facility, tool joint Set C multi-cycle testing was limited to 3 make and break cycles. Visual and dimensional inspection was performed on each connection after completing the multi-cycle make and break test, refer to Appendix D for inspection report. The purpose of the inspection was to document dimensions on select features susceptible to change (deformation) due to application of makeup torque and to ensure the connections were in acceptable condition for the torque to yield test. Minor dimensional changes had occurred to some features; however, all features were within new product specified dimensional requirements. Refer to Attachment A for photographs of the tool joints after completing the muti-cycle torque test. Light galls were detected on the thread load flank of Set A pin after six cycles at 63,980 ft-lb aim makeup torque. An attempt was made to repair the damage with a nonmetallic buffing wheel. (It is noted the equipment available to use for repair was not ideally suited for dressing threads, and no anti-gall solution was available to treat the repaired areas.) After repair, three additional make and break cycles were performed on tool joint Set A using 63,980 ft-lb aim makeup torque. The tool joint set was reinspected after the third make and break cycle and the light thread gall damage had redeveloped on the pin connection. Due to the damage, it was decided not to use tool joint Set A for a torque to yield test because the damage might produce misleading test results. No visible damage was observed on the secondary shoulder of any connections. A very light gall, roughness, was detected in an isolated area at the extreme outside edge of the seal shoulder on Box D.

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PTech+™ 52 Torque-Turn Test MTS, Waller-Tx, 27-April-2023 Page 5 of 5 The roughness was considered acceptable and no repair was necessary. No visible damage was detected on the seal shoulder of any other connection. Light burnishing, roughness, was detected on some thread flanks. The condition was considered to be normal wear from repeated make and break cycles. Test Results, Torque to Yield: During tool joint Set B torque to yield test, the maximum applied torque was inadvertently stopped at approximately 86,671 ft-lb. After consulting with MTS management, approval was granted to set the hydraulic bucking unit at its peak rated torque output of 105,000 ft-lb. The peaking torque setting was used for the torque to yield test performed on tool joint Set C and D. A summary of the torque to yield test data is shown in the below table. Peak Ratio Internal Applied Peak Breakout Tool Shoulder Makeup Breakout to Joint Gap Torque Torque Makeup Set (in) (ft-lb) (ft-lb) (%) A 0.0074 - - - B 0.0094 89,671 71,424 79.7 C 0.0086 104,185 80,308 77.1 D 0.0080 105,321 79,782 75.8 Set A torque to yield test not performed due to pin thread damage that occurred during the multi-cycle make and break test. Internal shoulder gap based on connection shoulder to shoulder length prior to start of torque to yield test, refer to Appendix D inspection report for connection length data. Connection calculated torsional yield = 91,400 ft-lb (1.0 FF). The torque to yield curve for each tool joint set is shown in Appendix F. For comparison purposes the tool joint sets are plotted on one chart. Refer to Attachment B for MTS torque-turn to yield curves for individual makeup and breakout cycles. Summary and Comments: The multi-cycle torque test shows the PTech+™ 52 connection breakout torque is consistently in the range of 75% to 80% of the applied makeup torque. The predicted breakout torque ratio for the connection is 79%. The predicted breakout torque ratio is a reference value calculated using the API torque formula modified with a negative value assigned to the useful work component. No significant change in the breakout torque ratio was observed during the multi-cycle make and break test. The results suggest the industry standard 3-cycle break in operation using the recommended makeup torque value is suitable for new drill pipe connections. No correlation was observed between the breakout torque ratio and change in shoulder position. The torque to yield test indicated consistent torque-turn performance for the tool joint sets. While the precise yield point cannot be identified on the torque-turn curve, the test does indicate the torsional capacity of the connection exceeds the calculated torsional yield.

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APPENDIX A Mechanical Test Data and Chemistry PTech+™ 52 Tool Joint Set A, B, C and D 6.625” OD x 3.750” ID x 135 ksi SMYS PTech+™ 52 Torque-Turn Test MTS, Waller-TX, 27-April-2023 Mechanical Test Data Pin Tool Joint, PTech+™ 52 Data Reported in JST Quality Documentation Package TSC P.O. 0274378-03 Tiger P.O. 2022-598 Rev-2 (QDP-2) Pin Tool Joint Tool Joint Serial No JST Representative Tool Joint Test No. Tensile Strength (psi) Yield Strength 0.2% offset (psi) Elongation 2” gage length (%) Reduction of Area (%) Charpy V-notch Impact (ft-lb) Hardness HBW Single Avg. OD Conn. A 22RN03541 22RN03515 161,572 149,050 17 58 60 69 77 69 337 325 B 22RN03739 22RN00539 159,058 146,101 17 58 73 79 78 77 337 321 C 22RN01259 22RN01295 161,234 148,374 16 58 65 63 69 66 337 341 D 22RN03727 22RN00539 159,058 146,101 17 58 73 79 78 77 337 321 Specified Requirement 140,000 min 135,000 min 165,000 max 13 min 45 min 40 min 285 to 341 Mechanical Test Data Box Tool Joint, PTech+™ 52 Data Reported in JST Quality Documentation Package TSC P.O. 0274378-03 Tiger P.O. 2022-598 Rev-2 (QDP-2) Box Tool Joint Tool Joint Serial No JST Representative Tool Joint Test No. Tensile Strength (psi) Yield Strength 0.2% Offset (psi) Elongation 2” gage length (%) Reduction of Area (%) Charpy V-notch Impact (ft-lb) Hardness HBW Single Avg. OD Conn. A 22RP03430 22RP02986 158,623 145,715 16 57 65 69 74 69 337 339 A (Mid-Wall Body Location) 160,847 148,229 17 58 66 68 63 66 B 22RP03210 22RP03320 157,414 143,732 17 59 79 77 70 75 309 326 C 22RP02780 22RP02802 159,300 146,536 18 60 66 72 66 68 309 337 D 22RP02784 22RP02802 Specified Requirement 140,000 min 135,000 min 165,000 max 13 min 45 min 40 min 285 to 341 Unless otherwise noted: - Box and Pin tool joint tensile and impact specimens secured from connection area, ref API Specification 5DP figure B13 - Box and Pin tool joint tensile specimen 0.5” round - Box and Pin tool joint Charpy V-notch test: longitudinal, 10 mm x 10 mm and -4°F Chemical Composition (wt%) Reported in JST Quality Documentation Package Heat No. C Si Mn P S Cr Ni Mo Cu E12209480XX 0.360 0.310 0.930 0.009 0.002 1.120 0.100 0.310 0.030 E22209327XX 0.360 0.300 0.920 0.009 0.001 1.130 0.100 0.310 0.030 E22211196AX 0.370 0.300 0.930 0.009 0.001 1.120 0.100 0.310 0.030 E22211197XX 0.360 0.310 0.940 0.008 0.001 1.130 0.100 0.310 0.020 TSC Spec 0.34 to 0.38 0.20 to 0.30 0.85 to 1.00 0.010 max 0.004 max 0.95 to 1.20 0.20 max 0.28 to 0.35 0.20 max Ca N Nb Ti Sn Sb As H (ppm) E12209480XX 0.001 0.0028 0.0139 0.010 0.002 0.001 0.003 0.7 E22209327XX 0.002 0.0031 0.0124 0.008 0.002 0.001 0.002 0.6 E22211196AX 0.002 0.0029 0.0127 0.010 0.002 0.001 0.002 0.5 E22211197XX 0.001 0.0029 0.0130 0.010 0.002 0.001 0.002 0.7 TSC Spec 0.001 to 0.006 0.009 max 0.020 max 0.005 to 0.010 0.015 max 0.008 max 0.008 max 2.0 max Heat E12209480XX: Pin A, Pin B and Pin D Heat E22209327XX: Pin C Heat E22211196AX: Box A and Box B Heat E22211197XX: Box C and Box D

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PTech+™ 52 Torque-Turn Test Page 1 of 1MTS, Waller-TX, 27-April-2023 Tool Joint Set A Cycles 1 thru 3: Aim MUT = 54,800 ft-lb (60% of TY) Cycles 4 thru 12: Aim MUT = 63,980 ft-lb (70% of TY) Cycle Count Makeup Torque (ft-lb) Breakout Torque (ft-lb) Ratio Breakout to Makeup Torque (%) Relative Position of Shoulders (in) 1 55,634 44,164 79.4 Punch Marks 3/3279.344,79556,47524/3280.044,60055,75334 64,696 51,919 80.3 9/32 5 65,005 52,030 80.0 12/32 6 65,214 51,158 78.4 14/32 7 65,352 51,901 79.4 15/32 8 64,375 52,296 81.2 16/32 9 65,354 50,220 76.8 18/32 20/3279.151,22564,7751020/3281.052,68465,0271112 64,752 51,390 79.4 20/32 Avg = 79.5 Tool Joint Set C Aim Makeup Torque = 54,800 ft-lb (60% of Calculated Torsional Yield) Cycle Count Makeup Torque (ft-lb) Breakout Torque (ft-lb) Ratio Breakout to Makeup Torque (%) Relative Position of Shoulders (in) 1 56,018 44,218 78.9 2 55,716 45,688 82.0 3 55,901 44,782 80.1 Punch Marks 4 55,303 43,327 78.3 2/32 5 56,001 44,386 79.3 0 6 55,761 45,275 81.2 2/32 3/3275.942,67456,25173/3277.142,90755,65689 55,958 43,036 76.9 5/32 10 55,395 43,959 79.4 5/32 11 55,485 43,014 77.5 6/32 12 55,083 42,607 77.4 4/32 13 55,740 43,164 77.4 5/32 14 55,739 42,933 77.0 5/32 5/3279.344,18055,72815 Avg = 78.5 Tool Joint Set B Aim Makeup Torque = 54,800 ft-lb (60% of Calculated Torsional Yield) Cycle Count Makeup Torque (ft-lb) Breakout Torque (ft-lb) Ratio Breakout to Makeup Torque (%) Relative Position of Shoulders (in) 1 56,236 45,486 80.9 Punch Marks 081.945,37055,39522/3281.345,47055,9343 Avg = 81.4 Tool Joint Set D Aim Makeup Torque = 54,800 ft-lb (60% of Calculated Torsional Yield) Cycle Count Makeup Torque (ft-lb) Breakout Torque (ft-lb) Ratio Breakout to Makeup Torque (%) Relative Position of Shoulders (in) 80.444,49855,3721Punch Marks 3/3276.842,92355,87123 55,452 42,143 76.0 5/32 4 55,830 42,718 76.5 5/32 5 55,460 43,222 77.9 7/32 6 55,128 41,388 75.1 8/32 7 55,521 41,320 74.4 10/32 8 55,976 41,498 74.1 10/32 9 56,233 42,347 75.3 12/32 55,175 10/3274.941,3191011 55,328 40,907 73.9 12/32 12 55,508 41,014 73.9 12/32 13 55,513 41,921 75.5 12/32 Avg = 75.8 Notes: 1. Jet-Lube KOPR EXT FF 1.0 thread compound (1.0 friction factor) used for all torque cycles. 2. Due to time constraint, Set B make and break test suspended prior to achieving three consecutive cycles with no relative change in position of shoulders. 3. Refer to Appendix D for connection dimensional inspection performed after completing multi-cycle torque test. APPENDIX CMulti-Cycle Torque Test Makeup and Breakout Data PTech+™ 52 Connection6.625” OD x 3.750” ID x 135 ksi SMYS

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PTech+™ 52 Torque-Turn TestMTS, Waller-TX, x-March-2023010,00020,00030,00040,00050,00060,00070,00080,00090,000100,000110,0000.600.550.500.450.400.350.300.250.200.150.100.050.00Applied Torque (ft-lb)TurnsTorque-Turn to Yield CurveTool Joint Set BTool Joint Set CTool Joint Set DRecommended Make-Up Torque = 54,800 ft-lb (60% of TY, 1.0 FF)Max Make-Up Torque = 63,980 ft-lb (70% of TY, 1.0 FF)Calculated Torsional Yield = 91,400 ft-lb (1.0 FF)PTech+™ 52 ConnectionTool Joint Sets: B, C and D6.625" OD x 3.750" ID x 135 ksi SMYSJet-Lube KOPR EXT FF 1.0 Thread CompoundHydraulic Bucking Unitlt050yiauqTxalyttevnqrorque inadvertentdieplpAlooootdeepuspended too soon on tosjoint Set B testAppendix D