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Coflore ATR Agitated Tube Reactor Pilot Scale Flow Reactor AM Technology Engineering Chemistry 1 www amt uk
AM Technology Company Overview Founded in 2000 AM Technology is a chemical engineering company based in Cheshire England that designs and maufactures the Coflore range of actively mixed continuous flow reactors for the chemical manufactring industry Whether for laboratory pilot or industrial scale chemical production our range of flow reactors offer a unique scope of capabilities suited towards a wide range of processes with wide ranging reaction times and reaction mixture types Coflore reactors are based on AM Technology s patented mixing technology which eliminates the need for drive shafts and rotary seals for improved ease of use cleaning and for added flexibilty versatility We also offer development services in our well equipped laboratory to carry out feasibility and scale up studies Certificate No 12073 ISO 9001 2015 2
Introduction Coflore continuous flow reactors are designed for flexibility scalability for processes with reaction times ranging from seconds to many hours The unique method of active mixing enables the processing of a wide versatile range of reaction mixtures including liquids gases and slurries The Coflore ATR is an actively mixed multi stage tubular reactor 0 35 mL to 10 L reactor volume achieving efficient mixing with a high degree of orderly flow irrespective of residence time AM Technology Engineering Chemistry T 44 0 1928 237420 E sales amt uk 3
Coflore ATR System The Coflore ATR system consists of an Agitating Platform Reactor Tube Assembly and Acoustic Cabinet ATR Reactor Tube Assembly can be configured in multiple arrangements which enables the volume of the reactor to be configured to suit the process requirements Reactor tubes can be disassembled to allow access for cleaning and testing of all wetted surfaces Agitating Platform provides horizontal agitation to the reactor tubes to generate mechanical mixing AM Technology Engineering Chemistry T 44 0 1928 237420 E sales amt uk 4
Coflore ATR Reactor Tube The Coflore ATR reactor tube consists of a Reactor Tube with Heat Transfer Jacket End Caps and an Agitator Agitators generate active mixing inside the reactor tube Active mixing decouples mixing and plug flow from residence time Agitators are interchangeable with different designs End Caps are used for connecting additional process inlets or temperature probes They can be removed to gain access for cleaning and testing of all wetted surfaces AM Technology Engineering Chemistry ATR Reactor Tubes are available in two sizes 0 35 L 1 25 L these are interchangeable Vertical reactor tube connections are used for process inlet outlet or reactor tube interconnections Heat Transfer Jacket consists of a spiral wound coil which transfers heating cooling through the reactor tube wall The heat transfer jackets are connected to the heat transfer manifold in either counter current or co current configurations T 44 0 1928 237420 E sales amt uk 5
Coflore ATR Reactor Tube Assembly The Coflore ATR Reactor Tube Assembly consists of a Reactor Tube Bank with Heat Transfer Jacket Manifold mounted on a reactor tube frame The Reactor Tube Frame is connected onto the agitation platform The reactor tube frame has multiple mounting holes enabaling various reactor tube configurations to be used with the same agitation platform Reactor Tubes can be connected to up to four tubes in a vertical cascade Two banks of reactor tubes can be mounted meaning up to 8 reactor tubes can be mounted on a reactor tube frame AM Technology Engineering Chemistry Heat Transfer Manifold provides heat transfer fluid to the ATR reactor tubes Valves are used for isolating regulating the heat transfer fluid flow T 44 0 1928 237420 E sales amt uk 6
Coflore ATR Reactor Tube Assembly The Coflore ATR Reactor Tube Assembly consists of a Reactor Tube Bank with Heat Transfer Jacket Manifold mounted on a reactor tube frame ATR Reactor Tube Assembly Operating Range 40 to 150 C up to 50 Bar Reactor tubes are interchangeable ATR reactor tubes can be removed for cleaning or to adjust reactor volume ATR reactor tubes have short vertical connections at each end enabling the reactor tubes to be close coupled together This provides minimal unmixed volume for the interstage channels AM Technology Engineering Chemistry T 44 0 1928 237420 E sales amt uk 7
Coflore ATR Inlet Outlet Connectors Reactor Tube End Caps have 1 2 triclover connections with a 9 5 mm ID inlet Custom design end caps with multiple connections are available on request 4 mm Triclover Adaptors1 adapt to a 1 4 BSPP with a 4 mm diameter through hole Can be used with 1 4 BSP injection plug to maintain deadspace and adapt to a 1 4 28 UNF thread Injection Plugs3 can be used to adapt from a 1 4 BSPP to 1 4 28 UNF thread 9 5 mm Triclover Adaptors2 adapt from a 1 2 triclover to a 1 4 BSPP with a 9 5 mm through hole Hose Barb Adaptors4 adapt from a 1 2 triclover to a hosebarb to suit a 4 8 mm ID tubing 1 AM Technology Engineering Chemistry 2 3 4 T 44 0 1928 237420 E sales amt uk 8
Coflore ATR Temperature Measurement A Thermowell sensor is used for temperature measurement within the ATR reactor tube Thermowells incorporate a T type thermocouple with miniature plug A Thermowell can be fitted to the ATR through the ATR reactor tube end cap Thermowells are recessed to provide accurate temperature measurement without affecting agitator travel AM Technology Engineering Chemistry T 44 0 1928 237420 E sales amt uk 9
Coflore ATR Agitating Platform The ATR agitating platform is mounted on an anti vibration table The ATR is available with either Analogue or Digital Control The ATR Cabinet provides noise insulation and protection from moving parts 4 OD Fume Extract Connection for connecting the ATR cabinet to local exhaust Removable Access Panels with viewing window and 1 4 turn panel key locks Removable to provide full access to the reactor tube assembly Bulkhead Connection Panels for mounting process hoses and connections Anti Vibration Table with removable enclosure panels for mounting peripherals Bolt Down Feet are used to secure the agitating platform and isolate vibration AM Technology Engineering Chemistry T 44 0 1928 237420 E sales amt uk 10
Coflore Analogue ATR Control Analogue ATR control incorporates the basic controls for operating the platform Control of the ATR is performed via a Local Control Panel on the anti vibration table Start Stop Agitation with push button Agitate Rate Select from 6 agitation frequencies with dial Frequencies 2 4 5 6 8 9 Hz Analogue control panel Temperature Display with up to 12 thermocouple inputs with one temperature display Select display temperature with selector switch AM Technology Engineering Chemistry T 44 0 1928 237420 E sales amt uk 11
Coflore ATR Digital Control Digital ATR control has a 5 5 interactive touchscreen enabling the user to control the platform and peripherals Digital ATR control is performed via a Remote Control Panel Digital Control Features include Temperature Display with up to 10 thermocouple inputs and 10 temperature displays Programmable Alarm for high and low temperature set points Ethernet Connection enabling remote control via PC Start Stop Agitation with 8 agitation frequencies 2 3 4 5 6 7 8 9 Hz Remote DCS PLC Interface for remote agitation control with local and remote emergency stop Pump Control for up to 3 pumps via a 4 20 mA signal to include start stop set point 0 100 pump flow rate totaliser automatic pump control Actuated Valve Control for up to 2 actuated valves to include open close time flow rate totaliser 4 20 mA Input Monitoring for to 4 input signals measuring 4 20 mA from 0 100 Data Logging for process monitoring data export to MS Excel ATEX certification and CFR21 compliance options available on request AM Technology Engineering Chemistry T 44 0 1928 237420 E sales amt uk 12
Coflore ATR Catalogue The Coflore ATR is a modular and easily customisable platform consisting of an Agitating Platform Control System Reactor Tube Assembly Acoustic Cabinet and Accessories Agitating Platform Control System Reactor Tube Assembly Accessories AM Technology Engineering Chemistry T 44 0 1928 237420 E sales amt uk 13
Coflore ATR Agitating Platforms Available as Analogue or Digital versions ATEX and CFR21 compliance available on request Analogue Agitating Platform ATR P100 Controls Agitation Start stop Agitate rate selection 2 4 5 6 8 9 Temperature 12 thermocouple input one display Size 1200 mm W 780 mm D 1800 mm H with cabinet Material 316 stainless steel Reactor mass 270 Kg total assembly Temp range 40 to 150 C Power 1ph N E 100 240 VAC 50 60 Hz 2A 2P E 16A 3 pin plug Compressed air 10mm push fit connection Air consumption 13 cfm at 7 bar oil free clean air Heat transfer 1 2 swagelok tube connection Single zone heat transfer manifold Digital Agitating Platform ATR P200 ATRP200 Ex Controls Agitation Start stop Agitate rate selection 2 3 4 5 6 7 8 9 Input output controls 10 x thermocouple input 10 x temperature display E stop circuit 3 x pump control output 2 x actuated valve control output 4 x 4 20 mA input 0 100 1 x digital input remote DCS PLC interface programmable alarm data logging export data to MS Excel remote control via ethernet supplied with 5 metre cable for connecting to ATR agitation platform Size 1200 mm W 780 mm D 1800 mm H with cabinet Material 316 stainless steel Reactor mass 270 Kg total assembly Temp range 40 to 150 C Power 1ph N E 100 240 VAC 50 60 Hz 2A 2P E 16A 3 pin plug Compressed air 10 mm push fit connection Air consumption 13 cfm at 7 bar oil free clean air Heat transfer 1 2 swagelok tube connection Single zone heat transfer manifold AM Technology Engineering Chemistry T 44 0 1928 237420 E sales amt uk 14
Coflore ATR Reactor Tubes Available in sizes 0 35 L or 1 25 L and materials 316 stainless steel or Hastelloy C276 Up to 8 reactor tubes per agitating platform 0 35 L Reactor Tube ATR 0 35L Ha ATR 0 35LSS Size 22 2 mm ID x 870 mm L Volume 0 35 L Wetted material Hastelloy C276 PTFE ATR 0 35LHa or 316 stainless steel PTFE ATR 0 35L SS Temp range 40 to 150 C Pressure Up to 50 Bar Connections 2 off 1 2 triclover connection per reactor tube end 1 off connection on end cap 1 off vertical connection per end Additional components include 1 off perforated tube agitator 16 x 865 mm L Available in 316 stainless steel or Hastelloy C276 1 25 L Reactor Tube ATR 1 25L Ha ATR 1 25LSS Size 42 7 mm ID x 870 mm L Volume 1 25 L Wetted material Hastelloy C276 PTFE ATR 1 25LHa or 316 stainless steel PTFE ATR 1 25L SS Temp range 40 to 150 C Pressure Up to 50 Bar Connections 2 off 1 2 triclover connection per reactor tube end 1 off connection on end cap 1 off vertical connection per end Additional components include 1 off perforated tube agitator 27 x 865 mm L Available in 316 stainless steel or Hastelloy C276 Available in 316 stainless steel or Hastelloy C276 AM Technology Engineering Chemistry T 44 0 1928 237420 E sales amt uk 15
Coflore ATR Accessories Accessories are available to meet your process requirements Acoustic Cabinet ATR Cabinet Provides noise insulation and protection from moving parts With fume extract connection and removable window panels for viewing and accessing the reactor tube assembly Size 1200 mm W 780 mm D 1800 mm H Material 304 Stainless steel Thermowell ATR TP Ha ATR TP SS T type thermocouple calibrated from 40 to 200 C Connections 1 2 triclover Wetted material Hastelloy C276 ATR TP Ha or 316 stainles steel ATR TP SS Thermowells incorporate a T type Thermocouple with miniature plug Inlet Outlet Hose ATR H 2000 Size 9 5 mm ID x 2000 mm PTFE braided hose Operating pressure Range up to 50 Bar Material 316 Stainless steel non wetted PTFE Connections 1 2 triclover Custom sizes available on request BSP Injection Plug ATR PLUG INJ BSP injection plug For use with 4mm triclover adaptor Adapts from BSP to 28 UNF Operating pressure range up to 10 Bar Material PTFE 316 Stainless steel non wetted Connections BSPP male 28 UNF female AM Technology Engineering Chemistry T 44 0 1928 237420 E sales amt uk 16
Coflore ATR Accessories Accessories are available to meet your process requirements Hose Barb Adaptor ATR HB Ha ATR HB SS Adapts from 1 2 triclover to hose barb Material Hastelloy C276 ATR HB Ha or 316 stainless steel ATR HB SS Connections 1 2 triclover 4 8 mm ID hose barb 4 mm Triclover Adaptor ATR BSP4 Ha ATRBSP4 SS Adapts 1 2 triclover to 1 4 BSP thread 4 mm through hole Can be used with 1 4 BSP injection plug Material Hastelloy C276 ATR BSP4 Ha or 316 Stainless steel ATR BSP4 SS Connections 1 2 triclover 1 4 BSP female 04 mm through hole 9 5 mm Triclover Adaptor ATR BSP9 5 Ha ATRBSP9 5 SS Adapts 1 2 triclover to 1 4 BSP thread 9 5mm through hole Material Hastelloy C276 ATR BSP9 5 Ha or 316 Stainless steel ATR BSP9 5 SS Connections 1 2 triclover 1 4 BSP female 09 5 mm through hole AM Technology Engineering Chemistry T 44 0 1928 237420 E sales amt uk 17
Coflore ATR Tool Kits Service Kits AM Technology recommends periodic maintainence using Tool kits and Service Kits to maintain optimum perfiornance of the Coflore ATR ATR Tool Kit ATR Tools Components include 1 x tool bag 1 x allen key set 1 x 17 mm ratchet spanner 2 x 13 mm spanners 2 x adjustable spanners 1 x pliers ATR Service Kits ATR Service Kit non ATEX ATR Service Kit EX ATEX Zone IICT4 Service and maintenance kit for the ATR Components include 1 x Solenoid Valve Assembly 4 x Pneumatic Actuator 4 x Agitation Springs Some of the agitating platform components have a limited life cycle The solenoid valve assembly pneumatic actuator and agitation springs should be replaced according to the following schedule Infrequent use less than 1 day per week Replace at user s discretion Frequent use 2 3 days per week Replace every 12 months Continuous use 5 days per week Replace every 6 months Continuous use 7 days per week Replace every 4 months In the event of the need to replace solenoids actuators or agitation springs please contact AM Technology AM Technology Engineering Chemistry T 44 0 1928 237420 E sales amt uk 18
Coflore ATR Gaskets Tube Fittings Gaskets are used to ensure a tight liquid and gas seal within the end cap flange of the ATR tube Available as Kits on request Tube fittings are used as process connections 1 2 Triclover Gasket Gk BS0050 PE PTFE envelope gasket Material PTFE Viton non wetted For use with ATR end caps ATR interconnections ATR PTFE hoses 1 Triclover Gasket Gk BS0100 PE PTFE envelope gasket Material PTFE Viton non wetted For use with 0 35 L ATR reactor tube 1 1 2 Triclover Gasket Gk BS10 0150 PE PTFE envelope gasket Material PTFE Viton non wetted For use with 1 25 L ATR reactor tube Soft Tubing Connector Soft tubing connectors for use with peristaltic pump tubing and BSP injection plug ATR PLUG INJ Material ETFE Connection 1 4 28 UNF male AM Technology Engineering Chemistry Master flex tubing size Tubing ID Barb size Part mm mm number L S 13 0 8 1 6 P 646 L S 14 1 6 1 6 P 646 L S 16 3 1 3 2 P 647 L S 25 4 8 4 8 P 648 T 44 0 1928 237420 E sales amt uk 19
Coflore ATR Tube Fittings Tube fittings are used as process connections Omifit Tube Connectors Omifit tube connectors for use with PTFE tubing and BSP injection plug ATR PLUG INJ Material Gripper body PEEK Ferrule PTFE Connections 28 UNF male Tubing size OD Part number 1 16 XP 283 1 8 XP 335 Swagelok Tube Connectors Swagelok tube connectors for use with PTFE Stainless steel tubing For use with 9 5 mm triclover adaptor ATR BSP9 5 Material Fitting 316 Stainless steel Washer Stainless steel viton Components include Compression fitting bonded washer AM Technology Engineering Chemistry Tubing size OD Part number 1 8 SS 200 1 4RP 1 4 SS 400 1 4RP T 44 0 1928 237420 E sales amt uk 20
Coflore ATR Technical Details Maximum reactor mass 120 kg Agitating platform mass 150 kg Noise 70 dBA Requirements Compressed air 3 7 bar 13 CFM oil free clean air Maximum air pressure 7 bar Power supply 1ph N E 100 240 VAC 50 60 Hz 2A Compressed air connection 10 mm push fit Heat transfer fluid connections 1 2 swagelock AM Technology Engineering Chemistry 1700 780 1800 1200 T 44 0 1928 237420 E sales amt uk 21
The Coflore Flow Reactor Range The entire range of Coflore Continuous Flow Reactors consists of the Agitated Cell Reactor ACR Agitated Tube Reactor ATR and the Rotating Tube Reactor RTR Facilitates laboratoryscale to full industrial scale production The Coflore ACR is an actively mixed ten stage system for efficient mixing and a high degree of orderly flow irrespective of residence time The Coflore ACR is a low volume reactor 30 mL to 100 mL which delivers comparable performance to the larger Coflore ATR RTR reactors The Coflore ATR is an actively mixed multi stage tubular reactor 0 35 mL to 10 L reactor volume achieving efficient mixing with a high degree of orderly flow irrespective of residence time The Coflore RTR operates as a tenstage actively mixed continuous flow reactor with a 100 L capacity that is capable of processing theoretically limitless reactor volumes without interruption AM Technology Engineering Chemistry T 44 0 1928 237420 E sales amt uk 22
Contact AM Technology We welcome enquiries from across the globe If you require more information about our reactors or to find out whether our reactors are suitable for any applications you have in mind we would be very interested in hearing from you Address AM Technology Unit 18 Berkeley Court Manor Park Runcorn Cheshire WA7 1TQ Telephone 44 0 1928 237420 Email sales amt uk Website www amt uk AM Technology Engineering Chemistry T 44 0 1928 237420 E sales amt uk 23
AM Technology Engineering Chemistry www amt uk